Synthesis and structure of a novel disulfide-containing aniline

Shi Ren Deng; Lei Wu; Hao Wang; Bin Zhou; Zao Ying Li; Yun Hong Zhou; Rick W K WONG; Jian Ping Guo

doi:10.1081/SCC-200046525

Synthesis and structure of a novel disulfide-containing aniline

Shi Ren Deng
, Lei Wu
, Hao Wang
, Bin Zhou
, Zao Ying Li^*
, Yun Hong Zhou
, Rick W K WONG
, Jian Ping Guo

^*Corresponding author for this work

Department of Chemistry

Research output: Contribution to journal › Journal article › peer-review

5 Citations (Scopus)

Abstract

A novel disulfide-containing aniline, 5,8-dihydro-1H,4H-2,3,6,7- tetrathiaanthracen-9-ylamine (6) was synthesized. The structures of the target compound and the intermediates have been identified by ¹H NMR, MS, IR, Raman and elemental analysis. In addition, the structure of 9-Nitro-5,8-dihydro-1H,4H-2,3,6,7-tetrathiaanthracene (5) was determined by single X-ray analysis.

Original language	English
Pages (from-to)	129-135
Number of pages	7
Journal	Synthetic Communications
Volume	35
Issue number	1
DOIs	https://doi.org/10.1081/SCC-200046525
Publication status	Published - 2005

User-Defined Keywords

Alkylbromination
Disulfide
Selective reduction
Thioesterification

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10.1081/SCC-200046525

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@article{8f575a0d001c4c57880fcdc3e14ec3c5,

title = "Synthesis and structure of a novel disulfide-containing aniline",

abstract = "A novel disulfide-containing aniline, 5,8-dihydro-1H,4H-2,3,6,7- tetrathiaanthracen-9-ylamine (6) was synthesized. The structures of the target compound and the intermediates have been identified by 1H NMR, MS, IR, Raman and elemental analysis. In addition, the structure of 9-Nitro-5,8-dihydro-1H,4H-2,3,6,7-tetrathiaanthracene (5) was determined by single X-ray analysis.",

keywords = "Alkylbromination, Disulfide, Selective reduction, Thioesterification",

author = "Deng, \{Shi Ren\} and Lei Wu and Hao Wang and Bin Zhou and Li, \{Zao Ying\} and Zhou, \{Yun Hong\} and WONG, \{Rick W K\} and Guo, \{Jian Ping\}",

note = "Funding Information: We gratefully acknowledge financial support by the National Natural Science Foundation of China (No. 29833090).",

year = "2005",

doi = "10.1081/SCC-200046525",

language = "English",

volume = "35",

pages = "129--135",

journal = "Synthetic Communications",

issn = "0039-7911",

publisher = "Taylor and Francis Ltd.",

number = "1",

}

TY - JOUR

T1 - Synthesis and structure of a novel disulfide-containing aniline

AU - Deng, Shi Ren

AU - Wu, Lei

AU - Wang, Hao

AU - Zhou, Bin

AU - Li, Zao Ying

AU - Zhou, Yun Hong

AU - WONG, Rick W K

AU - Guo, Jian Ping

N1 - Funding Information: We gratefully acknowledge financial support by the National Natural Science Foundation of China (No. 29833090).

PY - 2005

Y1 - 2005

N2 - A novel disulfide-containing aniline, 5,8-dihydro-1H,4H-2,3,6,7- tetrathiaanthracen-9-ylamine (6) was synthesized. The structures of the target compound and the intermediates have been identified by 1H NMR, MS, IR, Raman and elemental analysis. In addition, the structure of 9-Nitro-5,8-dihydro-1H,4H-2,3,6,7-tetrathiaanthracene (5) was determined by single X-ray analysis.

AB - A novel disulfide-containing aniline, 5,8-dihydro-1H,4H-2,3,6,7- tetrathiaanthracen-9-ylamine (6) was synthesized. The structures of the target compound and the intermediates have been identified by 1H NMR, MS, IR, Raman and elemental analysis. In addition, the structure of 9-Nitro-5,8-dihydro-1H,4H-2,3,6,7-tetrathiaanthracene (5) was determined by single X-ray analysis.

KW - Alkylbromination

KW - Disulfide

KW - Selective reduction

KW - Thioesterification

UR - https://www.scopus.com/pages/publications/13944252820

U2 - 10.1081/SCC-200046525

DO - 10.1081/SCC-200046525

M3 - Journal article

AN - SCOPUS:13944252820

SN - 0039-7911

VL - 35

SP - 129

EP - 135

JO - Synthetic Communications

JF - Synthetic Communications

IS - 1

ER -

Synthesis and structure of a novel disulfide-containing aniline

Abstract

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