Enrichment and determination of sixteen trace polycyclic aromatic hydrocarbons in barbecue smoke by using a continuous magnetic solid-phase extraction and gas chromatography-mass spectrometry

Yan Pan; Yanhao Zhang; Zifang Peng; Xin Ba; Wuduo Zhao; Xinglin Li; Yun Guo; Gangfeng Ouyang; Shusheng Zhang; Bin Zhang

doi:10.1002/sscp.201900068

Enrichment and determination of sixteen trace polycyclic aromatic hydrocarbons in barbecue smoke by using a continuous magnetic solid-phase extraction and gas chromatography-mass spectrometry

Yan Pan, Yanhao Zhang, Zifang Peng, Xin Ba, Wuduo Zhao^*, Xinglin Li, Yun Guo, Gangfeng Ouyang, Shusheng Zhang, Bin Zhang

^*Corresponding author for this work

Research output: Contribution to journal › Journal article › peer-review

5 Citations (Scopus)

Abstract

In this study, an innovative approach is proposed to predict the contribution of sixteen polycyclic aromatic hydrocarbons in barbecue smoke based on magnetic solid-phase extraction system and gas chromatography-mass spectrometry. In order to improve the detection limit of gas chromatography-mass spectrometry, a kinds of magnetic nanomaterial synthesized previously was used as a sorbent in magnetic solid-phase extraction. The recoveries ranged from 73.4% to 90.7%, and the limits of detection and limits of quantification were in the range 1.2-5.4 ng·L⁻¹ and 3.7-16.4 ng·L⁻¹ respectively. The method was successfully applied to the analysis of polycyclic aromatic hydrocarbons in smoke of the pork belly. The developed method could be potentially used for the assessing of polycyclic aromatic hydrocarbons profiles in environment pollution.

Original language	English
Pages (from-to)	28-36
Number of pages	9
Journal	Separation Science Plus
Volume	3
Issue number	1-2
DOIs	https://doi.org/10.1002/sscp.201900068
Publication status	Published - Jan 2020

User-Defined Keywords

gas chromatography-mass spectrometry
magnetic solid-phase extraction
polycyclic aromatic hydrocarbons

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This output contributes to the following UN Sustainable Development Goals (SDGs)

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10.1002/sscp.201900068

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Pan, Y., Zhang, Y., Peng, Z., Ba, X., Zhao, W., Li, X., Guo, Y., Ouyang, G., Zhang, S., & Zhang, B. (2020). Enrichment and determination of sixteen trace polycyclic aromatic hydrocarbons in barbecue smoke by using a continuous magnetic solid-phase extraction and gas chromatography-mass spectrometry. Separation Science Plus, 3(1-2), 28-36. https://doi.org/10.1002/sscp.201900068

@article{ea0a0d7d1c334c90b2c0f187d9290fb8,

title = "Enrichment and determination of sixteen trace polycyclic aromatic hydrocarbons in barbecue smoke by using a continuous magnetic solid-phase extraction and gas chromatography-mass spectrometry",

abstract = "In this study, an innovative approach is proposed to predict the contribution of sixteen polycyclic aromatic hydrocarbons in barbecue smoke based on magnetic solid-phase extraction system and gas chromatography-mass spectrometry. In order to improve the detection limit of gas chromatography-mass spectrometry, a kinds of magnetic nanomaterial synthesized previously was used as a sorbent in magnetic solid-phase extraction. The recoveries ranged from 73.4% to 90.7%, and the limits of detection and limits of quantification were in the range 1.2-5.4 ng·L−1 and 3.7-16.4 ng·L−1 respectively. The method was successfully applied to the analysis of polycyclic aromatic hydrocarbons in smoke of the pork belly. The developed method could be potentially used for the assessing of polycyclic aromatic hydrocarbons profiles in environment pollution.",

keywords = "gas chromatography-mass spectrometry, magnetic solid-phase extraction, polycyclic aromatic hydrocarbons",

author = "Yan Pan and Yanhao Zhang and Zifang Peng and Xin Ba and Wuduo Zhao and Xinglin Li and Yun Guo and Gangfeng Ouyang and Shusheng Zhang and Bin Zhang",

note = "Funding Information: Henan Province outstanding scientific and technological innovation talent. Grant Number: 184200510019 National Natural Science Foundation of China. Grant Numbers: 21775140, 21705143 Publisher Copyright: {\textcopyright} 2020 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim",

year = "2020",

month = jan,

doi = "10.1002/sscp.201900068",

language = "English",

volume = "3",

pages = "28--36",

journal = "Separation Science Plus",

issn = "2573-1815",

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}

Pan, Y, Zhang, Y, Peng, Z, Ba, X, Zhao, W, Li, X, Guo, Y, Ouyang, G, Zhang, S & Zhang, B 2020, 'Enrichment and determination of sixteen trace polycyclic aromatic hydrocarbons in barbecue smoke by using a continuous magnetic solid-phase extraction and gas chromatography-mass spectrometry', Separation Science Plus, vol. 3, no. 1-2, pp. 28-36. https://doi.org/10.1002/sscp.201900068

Enrichment and determination of sixteen trace polycyclic aromatic hydrocarbons in barbecue smoke by using a continuous magnetic solid-phase extraction and gas chromatography-mass spectrometry. / Pan, Yan; Zhang, Yanhao; Peng, Zifang et al.
In: Separation Science Plus, Vol. 3, No. 1-2, 01.2020, p. 28-36.

Research output: Contribution to journal › Journal article › peer-review

TY - JOUR

T1 - Enrichment and determination of sixteen trace polycyclic aromatic hydrocarbons in barbecue smoke by using a continuous magnetic solid-phase extraction and gas chromatography-mass spectrometry

AU - Pan, Yan

AU - Zhang, Yanhao

AU - Peng, Zifang

AU - Ba, Xin

AU - Zhao, Wuduo

AU - Li, Xinglin

AU - Guo, Yun

AU - Ouyang, Gangfeng

AU - Zhang, Shusheng

AU - Zhang, Bin

N1 - Funding Information: Henan Province outstanding scientific and technological innovation talent. Grant Number: 184200510019 National Natural Science Foundation of China. Grant Numbers: 21775140, 21705143 Publisher Copyright: © 2020 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim

PY - 2020/1

Y1 - 2020/1

N2 - In this study, an innovative approach is proposed to predict the contribution of sixteen polycyclic aromatic hydrocarbons in barbecue smoke based on magnetic solid-phase extraction system and gas chromatography-mass spectrometry. In order to improve the detection limit of gas chromatography-mass spectrometry, a kinds of magnetic nanomaterial synthesized previously was used as a sorbent in magnetic solid-phase extraction. The recoveries ranged from 73.4% to 90.7%, and the limits of detection and limits of quantification were in the range 1.2-5.4 ng·L−1 and 3.7-16.4 ng·L−1 respectively. The method was successfully applied to the analysis of polycyclic aromatic hydrocarbons in smoke of the pork belly. The developed method could be potentially used for the assessing of polycyclic aromatic hydrocarbons profiles in environment pollution.

AB - In this study, an innovative approach is proposed to predict the contribution of sixteen polycyclic aromatic hydrocarbons in barbecue smoke based on magnetic solid-phase extraction system and gas chromatography-mass spectrometry. In order to improve the detection limit of gas chromatography-mass spectrometry, a kinds of magnetic nanomaterial synthesized previously was used as a sorbent in magnetic solid-phase extraction. The recoveries ranged from 73.4% to 90.7%, and the limits of detection and limits of quantification were in the range 1.2-5.4 ng·L−1 and 3.7-16.4 ng·L−1 respectively. The method was successfully applied to the analysis of polycyclic aromatic hydrocarbons in smoke of the pork belly. The developed method could be potentially used for the assessing of polycyclic aromatic hydrocarbons profiles in environment pollution.

KW - gas chromatography-mass spectrometry

KW - magnetic solid-phase extraction

KW - polycyclic aromatic hydrocarbons

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DO - 10.1002/sscp.201900068

M3 - Journal article

AN - SCOPUS:85147399840

SN - 2573-1815

VL - 3

SP - 28

EP - 36

JO - Separation Science Plus

JF - Separation Science Plus

IS - 1-2

ER -

Enrichment and determination of sixteen trace polycyclic aromatic hydrocarbons in barbecue smoke by using a continuous magnetic solid-phase extraction and gas chromatography-mass spectrometry

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